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TSKgel SuperH Columns

The TSKgel SuperH column line consists of eight columns with different pore sizes, TSKgel SuperH1000 through TSKgel SuperH7000, and four columns with an extended linear range of the calibration curve. The calibration curves are shown below.
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TSKgel SuperH Columns

The TSKgel SuperH column line consists of eight columns with different pore sizes, TSKgel SuperH1000 through TSKgel SuperH7000, and four columns with an extended linear range of the calibration curve. The calibration curves are shown below.

TSKgel SuperH-type columns are high efficiency/high throughput versions of the conventional TSKgel Hhr columns. Both column types are based on the same bead chemistry.

Main characteristics:

Maximum operating temperature for TSKgel SuperH-type columns is 140 °C.

Broad solvent range. All TSKgel SuperH-type columns are shipped in THF, which can be exchanged for a wide variety of organic solvents, as is shown below.

TSKgel SuperH-type columns are high efficiency, high-throughput gel permeation(HT-GPC) columns with dimensions of 6 mm ID x 15 cm.

Figure 1: Calibration Curves on TSKgel SuperH Columns

Greenherbs

Beware of extra-column bandbroadening

The volume of a TSKgel SuperH column is 3.4 times smaller than that of a conventional 7.8mm x 30cm column. As a result, peak volumes will be proportionally smaller on TSKgel SuperH-type columns compared to a corresponding TSKgel Hhr column. Thus, your HPLC system may require optimization of components that can give rise to extra-column bandbroadening, such as connecting tubing, injector, injection volume, detector cell volume, and detector time constant.

Columns with linear calibration curves

The TSKgel SuperH product line contains four linear or mixed-bed columns, in which particles with different pore sizes are blended to provide an extended linear calibration curve. The mixed-bed columns feature increasing linear calibration ranges, from TSKgel SuperHM-L, SuperHM-N, SuperHM-M, to SuperHM-H.

Shipping Solvent

Can Be Replaced With

Tetrahydrofuran

acetone, ethanol, quinoline, benzene, o-dichlorobenzene, ethyl acetate,
dodecane, FC-113, carbon tetrachloride5, dichloromethane,
dichloroethane, trichloroethane, n-hexane, cyclohexane,
xylene, tetrahydrofuran, chloroform, 1,4-dioxane,
hexafluoroisopropanol, toluene, 1-chloronaphthalene,
dimethylaceto acetamide, methyl ethyl ketone, trichlorobenzene,
m-cresol, dimethylformamide, methylpyrrolidone,
o-chlorophenol/chloroform, dimethyl sulfoxide, pyridine

Notes:

1、In case of TSKgel SuperH and HHR, see table below for appropriate flow rates for solvent exchange. After switching to a very polar solvent, switching to a nonpolar is not recommended.

2、All TSKgel HXL, HHR, SuperHZ and SuperH analytical columns are shipped containing tetrahydrofuran(THF), except High Temperature(HT) columns, which contain o-dichlorobenzene.

3、Prolonged exposure to carbon tetrachloride can corrode the stainless steel parts of a column and an HPLC system.

* 100% methanol cannot be used with TSKgel H-type columns; use this solvent with TSKgel SW-type or Alpha-type columns.

** TSKgel H columns may be specially ordered with this shipping solvent.

Solvent

Recommended Flow Rate

n-Hexane

0.9

methyl ethyl ketone

0.7

dichloromethane, ethyl acetate

0.6

toluene, chloroform

0.5

dimethylformamide

0.4

carbon tetrachloride, pyridine

0.3

dimethyl sulfoxide, dioxane, ethanol,
N-methylpyrrolidone, o-dichlorobenzene

0.2

quinoline, hexafluoroisopropanal,
1-chloronaphthalene

0.1

Recommended Solvent

Application

THF

polystyrene, epoxy resin, phenoxy resin, polycarbonate,
polyisoprene, polyvinyl acetate, polyvinyl chloride,
monoglycerides, fatty acids, poly(butadiene),
polybutadiene, poly(methyl methacrylate),
poly(styrene-butadiene), poly(styrene-acrylonitrile)

N,N-Dimethylformamide(DMF) +/- 5mM LiBr

polyvinyl chloride, polyvinyl fluoride, urea resins,
polyurethane, polystyrene, polyester,
polyimido ether, polyimido ester,
polyphenol(aqueous solution), polyacrylonitrile

o-Dichlorobenzene(ODCB)

polyethylene, polypropylene

Chloroform

polycarboxylic ether, acrylic resin,
epoxy resin, polystyrene

m-Cresol/Chloroform

nylon, polyester, polyamide,
poly(ethylene terephthalate)

Toluene

polybutadiene, polysiloxane

TSKgel SuperH1000

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

1.5 nm

Exclusion Limit:

1,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017990

TSKgel SuperH1000

3 µm

Stainless Steel

6

15

0018002

Guard Column for P/N 0017990

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperH2000

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

2.0 nm

Exclusion Limit:

10,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017991

TSKgel SuperH2000

3 µm

Stainless Steel

6

15

0018002

Guard Column for P/N 0017991

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperH2500

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

3.0 nm

Exclusion Limit:

20,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017992

TSKgel SuperH2500

3 µm

Stainless Steel

6

15

0018002

Guard Column for P/N 0017992

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperH3000

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

7.5 nm

Exclusion Limit:

60,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017993

TSKgel SuperH3000

3 µm

Stainless Steel

6

15

0018002

Guard Column for P/N 0017993

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperH4000

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

2.0 nm

Exclusion Limit:

400,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017994

TSKgel SuperH4000

3 µm

Stainless Steel

6

15

0018002

Guard Column for P/N 0017994

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperH5000

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

6.5 nm

Exclusion Limit:

4 x 106 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017995

TSKgel SuperH5000

3 µm

Stainless Steel

6

15

0018003

Guard Column for P/N 0017995

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperH6000

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

ND

Exclusion Limit:

4 x 107 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017996

TSKgel SuperH6000

5 µm

Stainless Steel

6

15

0018003

Guard Column for P/N 0017996

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperH7000

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

ND

Exclusion Limit:

4 x 108 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017997

TSKgel SuperH7000

5 µm

Stainless Steel

6

15

0018003

Guard Column for P/N 0017997

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperHM-H

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm & 5 µm

Pore size(mean):

mixed

Exclusion Limit:

4 x 108 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0018001

TSKgel SuperHM-H

3 & 5 µm

Stainless Steel

6

15

0018003

Guard Column for P/N 0018001

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperHM-M

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

mixed

Exclusion Limit:

4 x 106 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0018000

TSKgel SuperHM-M

3 µm

Stainless Steel

6

15

0018003

Guard Column for P/N 0018000

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperHM-N

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

mixed

Exclusion Limit:

4 x 105 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017999

TSKgel SuperHM-N

3 µm

Stainless Steel

6

15

0018003

Guard column for P/N 0017999

3 µm

Stainless Steel

4.6

3.5

TSKgel SuperHM-L

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

3 µm

Pore size(mean):

mixed

Exclusion Limit:

4 x 106 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017998

TSKgel SuperHM-L

3 µm

Stainless Steel

6

15

0018003

Guard Column for P/N 0017998

3 µm

Stainless Steel

4.6

3.5

We could not find any corresponding parameters, please add them to the properties table

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