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TSKgel HHR Columns for Expanded Solvent Capability

The TSKgel HHR column line consists of eight columns with different pore sizes, TSKgel G1000HHR through TSKgel G7000HHR, and five columns with an extended linear range of the calibration curve. The calibration curves are shown below.
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Description
Parameters

TSKgel HHR Columns for Expanded Solvent Capability

The TSKgel HHR column line consists of eight columns with different pore sizes, TSKgel G1000HHR through TSKgel G7000HHR, and five columns with an extended linear range of the calibration curve. The calibration curves are shown below.

Main characteristics

Maximum operating temperature for TSKgel HHR-type columns is 140 ºC.

Broad solvent range. All TSKgel HHR-type columns are shipped in THF, which can be exchanged for a wide variety of organic solvents as shown below.

TSKgel HHR-type columns are conventional GPC columns with dimensions of 7.8 mm ID x 30 cm. Most HPLC systems do not require optimization of extra-column bandbroadening effects when working with conventional GPC columns.

Calibration Curves on TSKgel HHR Columns

Greenherbs

Shipping Solvent

Can Be Replaced With

Tetrahydrofuran

acetone, ethanol, quinoline, benzene, o-dichlorobenzene, ethyl acetate,
dodecane, FC-113, carbon tetrachloride5, dichloromethane,
dichloroethane, trichloroethane, n-hexane, cyclohexane,
xylene, tetrahydrofuran, chloroform, 1,4-dioxane,
hexafluoroisopropanol, toluene, 1-chloronaphthalene,
dimethylaceto acetamide, methyl ethyl ketone, trichlorobenzene,
m-cresol, dimethylformamide, methylpyrrolidone,
o-chlorophenol/chloroform, dimethyl sulfoxide, pyridine

Notes:

1、In case of TSKgel SuperH and HHR, see table below for appropriate flow rates for solvent exchange. After switching to a very polar solvent, switching to a nonpolar is not recommended.

2、All TSKgel HXL, HHR, SuperHZ and SuperH analytical columns are shipped containing tetrahydrofuran(THF), except High Temperature(HT) columns, which contain o-dichlorobenzene.

3、Prolonged exposure to carbon tetrachloride can corrode the stainless steel parts of a column and an HPLC system.

* 100% methanol cannot be used with TSKgel H-type columns; use this solvent with TSKgel SW-type or Alpha-type columns.

** TSKgel H columns may be specially ordered with this shipping solvent.

Columns with linear calibration curves

The TSKgel HHR product line contains five linear, or mixed-bed columns, in which particles with different pore sizes are blended to provide an extended linear calibration curve. The mixe-bed columns feature increasing linear calibration ranges, from TSKgel GMHHR-L, GMHHR-N, GMHHR-M, to GMHHR-H. TSKgel GMHHR-H(S) HT is a high temeperature mixed bed column shipped in ODCB, o-dichlorobenzene.

Solvent

Recommended Flow Rate

n-Hexane

0.9

methyl ethyl ketone

0.7

dichloromethane, ethyl acetate

0.6

toluene, chloroform

0.5

dimethylformamide

0.4

carbon tetrachloride, pyridine

0.3

dimethyl sulfoxide, dioxane, ethanol,
N-methylpyrrolidone, o-dichlorobenzene

0.2

quinoline, hexafluoroisopropanal,
1-chloronaphthalene

0.1

Recommended Solvent

Application

THF

polystyrene, epoxy resin, phenoxy resin, polycarbonate,
polyisoprene, polyvinyl acetate, polyvinyl chloride,
monoglycerides, fatty acids, poly(butadiene),
polybutadiene, poly(methyl methacrylate),
poly(styrene-butadiene), poly(styrene-acrylonitrile)

N,N-Dimethylformamide(DMF) +/- 5mM LiBr

polyvinyl chloride, polyvinyl fluoride, urea resins,
polyurethane, polystyrene, polyester,
polyimido ether, polyimido ester,
polyphenol(aqueous solution), polyacrylonitrile

o-Dichlorobenzene(ODCB)

polyethylene, polypropylene

Chloroform

polycarboxylic ether, acrylic resin,
epoxy resin, polystyrene

m-Cresol/Chloroform

nylon, polyester, polyamide,
poly(ethylene terephthalate)

Toluene

polybutadiene, polysiloxane

TSKgel G1000HHR

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

1.5 nm

Exclusion Limit:

< 1,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF for 0017352 and 0017368

Chloroform for 0018270 and 0018271

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017352

TSKgel G1000HHR

5 µm

Stainless Steel

7.8

30

0017368

Guard Column for P/N 0017352

5 µm

Stainless Steel

6

4

0018270

TSKgel G1000HHR

5 µm

Stainless Steel

21.5

30

0018271

Guard Column for P/N 0018270

5 µm

Stainless Steel

7.5

7.5

TSKgel G2000HHR

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

2 nm

Exclusion Limit:

< 10,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF for 0017353 and 0017368

Chloroform for 0018259 and 0018271

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017353

TSKgel G2000HHR

5 µm

Stainless Steel

7.8

30

0017368

Guard Column for P/N 0017353

5 µm

Stainless Steel

6

4

0018259

TSKgel G2000HHR

5 µm

Stainless Steel

21.5

30

0018271

Guard Column for P/N 0018259

5 µm

Stainless Steel

7.5

7.5

TSKgel G2500HHR

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

3 nm

Exclusion Limit:

20,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF for 0017354 and 0017368

Chloroform for 0018266 and 0018271

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017354

TSKgel G2500HHR

5 µm

Stainless Steel

7.8

30

0017368

Guard Column for P/N 0017354

5 µm

Stainless Steel

6

4

0018266

TSKgel G2500HHR

5 µm

Stainless Steel

21.5

30

0018271

Guard Column for P/N 0018266

5 µm

Stainless Steel

7.5

7.5

TSKgel G3000HHR

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

7.5 nm

Exclusion Limit

60,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF for 0017355 and 0017368

Chloroform for 0018267 and 0018271

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017355

TSKgel G3000HHR

5 µm

Stainless Steel

7.8

30

0017368

Guard Column for P/N 0017355

5 µm

Stainless Steel

6

4

0018267

TSKgel G3000HHR

5 µm

Stainless Steel

21.5

30

0018271

Guard Column for P/N 0018267

5 µm

Stainless Steel

7.5

7.5

TSKgel G4000HHR

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

20 nm

Exclusion Limit:

< 400,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF for 0017356 and 0017368

Chloroform for 0018268 and 0018271

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017356

TSKgel G4000HHR

5 µm

Stainless Steel

7.8

30

0017368

Guard Column for P/N 0017356

5 µm

Stainless Steel

6

4

0018268

TSKgel G4000HHR

5 µm

Stainless Steel

21.5

30

0018271

Guard Column for P/N 0018268

5 µm

Stainless Steel

7.5

7.5

TSKgel G5000HHR

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

65 nm

Exclusion Limit:

< 4 x 106 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017357

TSKgel G5000HHR

5 µm

Stainless Steel

7.8

30

0017369

Guard Column for P/N 0017357

5 µm

Stainless Steel

6

4

TSKgel G6000HHR

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

ND

Exclusion Limit:

< 4 x 107 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017358

TSKgel G6000HHR

5 µm

Stainless Steel

7.8

30

0017369

Guard Column for P/N 0017358

5 µm

Stainless Steel

6

4

TSKgel G7000HHR

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

ND

Exclusion Limit:

4 x 108 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017359

TSKgel G7000HHR

5 µm

Stainless Steel

7.8

30

0017369

Guard Column for P/N 0017359

5 µm

Stainless Steel

6

4

TSKgel GMHHR-H mixed-bed

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

ND

Exclusion Limit:

< 4 x 108 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF for 0017360 and 0017369

Chloroform for 0018269 and 0018272

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017360

TSKgel GMHHR-H

5 µm

Stainless Steel

7.8

30

0017369

Guard column for P/N 0017360

5 µm

Stainless Steel

6

4

0018269

TSKgel GMHHR-H

5 µm

Stainless Steel

21.5

30

0018272

Guard column for P/N 0018269

5 µm

Stainless Steel

7.5

7.5

TSKgel GMHHR-M mixed bed

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

mixed

Exclusion Limit:

< 4 x 106 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017392

TSKgel GMHHR-M

5 µm

Stainless Steel

7.8

30

0017369

Guard Column for P/N 0017392

5 µm

Stainless Steel

6

4

TSKgel GMHHR-N

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

mixed

Exclusion Limit:

< 400,000 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0018055

TSKgel GMHHR-N

5 µm

Stainless Steel

7.8

30

0017369

Guard Column for P/N 0018055

5 µm

Stainless Steel

6

4

TSKgel GMHHR-L mixed bed

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

5 µm

Pore size(mean):

mixed

Exclusion Limit:

4 x 106 Da

Max. Temp.(ºC):

140

Shipping Solvent:

THF

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0017362

TSKgel GMHHR-L

5 µm

Stainless Steel

7.8

30

0017369

Guard Column for P/N 0017362

5 µm

Stainless Steel

6

4

TSKgel GMHHR-H(S) HT mixed bed

Matrix:

polystyrene-divinylbenzene

Particle Size(mean):

13 µm

Pore size(mean):

mixed

Exclusion Limit:

< 4 x 108 Da

Max. Temp.(ºC):

140

Shipping Solvent:

ODCB

P/N

Description

Particle size

Housing material

ID(mm)

Length(cm)

0018393

TSKgel GMHHR-H(S) HT

13 µm

Stainless Steel

7.8

30

0018397

Guard column for P/N 0018393

13 µm

Stainless Steel

7.5

7.5
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